Two parts as I suggested.
Measure mains by themselves. if the dip is there then you know it's them. If its not, then its an interaction between the Mains and Sub. Tracking it can be frustrating.
One of my towers had a 20dB suckout. I was trying to figure out why it had the null and my other did not. I was in conversation with somebody when I got the idea to look at the wavelength for that frequency. As I was coming to the realization that it was a cancellation due to that frequency wavelength bouncing off the back wall, he was hitting me up with a comment about Wilson Audio always having their display speakers slightly off kilter. I changed that Left Main by about 1.5" from the front and slightly changed the toe angle and the suckout disappeared, becoming a standard LF dip.