Still at it, I see.
First, you're not trying to diffuse sound, you're trying to absorb it- if you want to diffuse it, add irregularly-shaped items and move them around the room so the sound impacts them early in the path.
I would start by using the RTA with each speaker separately. One is likely to be different from another in its response and as the other is added gradually (using the balance control), the dip around 72Hz will show up, indicating that it's a cancellation caused by speaker placement. While it's not reasonable to expect drastic changes in placement, small ones can make a big difference. I would mark the speaker location with painter's tape at the corners, then adjust the toe-in. LISTEN before making any other changes but measure it again.
I had a big cancellation in my room closer to 80Hz and it was so bad I hated listening because the furniture can't really be moved and I didn't want to rotate the room/system. I ran Room EQ Wizard and saw the problem, so I rotated the speakers as I mentioned. It helped, but more for the overall image/separation than the problem. Then, because I had them left over from a home theater demo, I started placing the acoustic panels I had made- began at the left side first reflection area and saw that it helped, but not much. Then, I added panels to the front corners and saw a strong change for the better. Next, I put a panel in the left rear corner and continued by stacking another on that one. The right rear corner is a doorway, so it can't have a panel, nor does it need one. I used 4" thick at the front corners and 2" at the rear, all are 2' x 4'. The problem is gone and I didn't spend much on these, which are 1" thick Owens-Corning 703 fiberglass, fastened to pegboard with contact cement, covered with muslin. The muslin was used because it's inexpensive and it blends in with the paint color. Any fabric that you can see through easily will work- you're not going to find something that's demonstrably better, even from Guilford of Maine (I have their catalog- it's nothing special).