Hey there Oliver,
A couple that I have and use are....
Alpine's, Highway One, I have found as extremely useful. It has a series of tracks that test for imaging, timbre, SPL, bass blur (can't think of the technical term), tweeter ability, plus have a few tests at the end like phase checks, white noise, noise floor and stereo imaging. I bought this from our local Home Theatre specialist.
Test cd's by Bass Mechanic. They specialise in bass for car systems typically but have released a couple of cd's with frequency test tones that start from 5 Hz and run up to 24 KHz. Perhaps a car audio dealer may have these.
I have found these to be good, but they are limited to tuning and tweaking by ear. So if you're tone deaf, they might not be your best choice, but if you have acute audio ears, then they should help you well.
You can get test cd's which use a microphone to auto calibrate, but I am not sure where from, plus the price is higher. Sorry
Happy tuning....
Ebay might be a good place to look....