I have a test tone disc that I use that sweeps through various frequencies from 16Hz to over 100Hz. You can also download those tones from the internet and make your own CD. My disc also has an initial track that is pink noise that I use to set the volume level on my receiver so that I read 70dB on my SPL meter (some people use higher, some use lower). After setting the volume control on the receiver, you would keep the volume on the receiver the same and record the SPL reading on the meter for the various frequencies (like you said). For the Radio Shack SPL meters, there are correction factors for the lower frequencies that you can download - I'm not sure about the other SPL meters. Some others here are more knowledgeable about that.
In Excel, you could make two columns of data. The first column would be the frequencies of the tones (and you'd just enter the value of the frequencies). The second column would be the SPL readings for those frequencies. You can also incorporate the correction factors in Excel. When you plot the data, the X axis would be frequency and the Y axis would be measured SPL.
As an example of a plot that I made this way, you can check out the attached plot of the first post in the thread linked
here.
That's just to get the ball rolling. I'll be happy to help you out more with this.